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2 article(s) from Nahra, Fady

Olefin metathesis in air

Lorenzo Piola,
Fady Nahra and
Steven P. Nolan

Beilstein J. Org. Chem. 2015, 11, 2038–2056, doi:10.3762/bjoc.11.221

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Graphical Abstract

Scheme 1: Polymerization of 7-oxanorbornene in water.

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Scheme 2: Synthesis of the first well-defined ruthenium carbene.

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Scheme 3: Synthesis of Grubbs' 1^st generation catalyst.

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Figure 1: NHC-Ruthenium complexes and widely used NHC carbenes.

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Scheme 4: Access to 21 from the Grubbs’ 1^st generation catalyst and its one-pot synthesis.

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Scheme 5: Synthesis of supported Hoveyda-type catalyst.

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Figure 2: Scope of RCM reactions with supported Hoveyda-type catalyst. Reaction conditions: 24 (5 mol %), non...

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Scheme 6: Synthesis of 33 by Hoveyda and Blechert.

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Figure 3: Synthesis of chiral Hoveyda–Grubbs type catalyst and its use in RO/CM.

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Scheme 7: Synthesis of 41.

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Figure 4: RCM reactions in air using 41 as catalyst. Reaction conditions: 41 (5 mol %), MeOH (0.05 M), 22 °C,...

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Figure 5: CM-type reactions in air using 41 as catalyst. Reaction conditions: 41 (5 mol %), 22 °C, 12 h, in a...

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Figure 6: Grela's complex (54) and reaction scope in air. Reaction conditions: catalyst, substrate (0.25 mmol...

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Figure 7: Abell's complex (61) and its RCM reaction scope in air. Reaction condition: 10 mol % of 61, refluxi...

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Figure 8: Catalysts used by Meier in air.

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Figure 9: Ammonium chloride-tagged complexes.

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Figure 10: Scorpio-type complexes.

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Scheme 8: Synthesis of Grubbs' 3^rd generation catalyst.

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Figure 11: Indenylidene complexes.

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Figure 12: Commercially available complexes evaluated under air.

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Figure 13: Grela's N,N-unsymmetrically substituted complexes.

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Scheme 9: Synthesis of phosphite-based catalysts.

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Figure 14: Catalysts used by the Cazin group.

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Figure 15: RCM scope in air with catalysts 33, 85 and 98a. Reaction conditions: Catalyst, substrate (0.25 mmol...

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Figure 16: Synthesis of Schiff base-ruthenium complexes.

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Scheme 10: Schiff base–ruthenium complexes synthesized by Verpoort.

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Scheme 11: Synthesis of mixed Schiff base–NHC complexes.

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Figure 17: Veerport's indenylidene Schiff-base complexes.

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Review

Published 30 Oct 2015

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Ruthenium indenylidene “1^st generation” olefin metathesis catalysts containing triisopropyl phosphite

Stefano Guidone,
Fady Nahra,
Alexandra M. Z. Slawin and
Catherine S. J. Cazin

Beilstein J. Org. Chem. 2015, 11, 1520–1527, doi:10.3762/bjoc.11.166

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Figure 1: Examples of ruthenium complexes used in olefin metathesis reactions.

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Scheme 1: Synthesis of the mixed phosphine/phosphite complex 1.

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Figure 2: Molecular structure of mixed phosphine/phosphite complex 1. Hydrogen atoms are omitted for clarity.

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Scheme 2: Synthesis of the bis-phosphite complex 2.

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Figure 3: Molecular structure of 2 and the ylide 3. Hydrogen atoms and solvent molecules are omitted for clar...

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Figure 4: Reaction profiles of mixed phosphine/phosphite 1 and phosphine-based Ind-I in the RCM of 4 (lines a...

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Full Research Paper

Published 01 Sep 2015

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Olefin metathesis in air

Ruthenium indenylidene “1st generation” olefin metathesis catalysts containing triisopropyl phosphite

Ruthenium indenylidene “1^st generation” olefin metathesis catalysts containing triisopropyl phosphite